C₂₅H₂₂N₂O₅

Base Information

Chemical Name:C₂₅H₂₂N₂O₅
CAS No.:792948-31-3
Molecular Formula:C₂₅H₂₂N₂O₅
Molecular Weight:430.46
Hs Code.:

C<sub>25</sub>H<sub>22</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₅H₂₂N₂O₅

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Chemical Property of C₂₅H₂₂N₂O₅

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Technology Process of C₂₅H₂₂N₂O₅

There total 16 articles about C₂₅H₂₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-vinyl-2,5-dihydro-1H-pyrrole-2-carboxylic acid methyl ester

: 792948-31-3
C₂₅H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1: 93 mg / Et₃N / CH₂Cl₂ / 12 h / 0 °C

2: Zn; AcOH / CH₂Cl₂ / 0.33 h / 20 °C

3: 451 mg / aq. HCl / tetrahydrofuran / 24 h / 20 °C

4: 91 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh / CH₂Cl₂ / 12 h / Heating

5: K₂CO₃ / methanol / 9 h / 0 °C

6: MnO₂ / CH₂Cl₂ / 72 h / 20 °C

7: aq. NaClO₂; KH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 3 h / 20 °C

8: 11 mg / SOCl₂ / 18 h / 20 °C

9: RuCl₃*3H₂O / 110 °C

10: CF₃CO₂H; BF₃*Et₂O / 0.17 h / 20 °C

11: 9 mg / TsOH / 40 h / 100 °C

With hydrogenchloride; manganese(IV) oxide; ruthenium trichloride; sodium chlorite; potassium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; acetic acid; triethylamine; trifluoroacetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.tet.2004.07.040

Reference yield:

: 792948-36-8
(S)-4-methylsulfanyl-2-prop-2-ynylaminobutyric acid methyl ester

: 792948-31-3
C₂₅H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 16 steps

1: 100 percent / aq. KHCO₃ / ethyl acetate / 14 h / 0 °C

2: 100 percent / aq. NaIO₄ / methanol / 4 h / 0 °C

3: 37 percent / xylene / 60 h / 140 °C

4: 76 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 24 h / 20 °C

5: TMSCl; NaI / acetonitrile / 10 h / 20 °C

6: 93 mg / Et₃N / CH₂Cl₂ / 12 h / 0 °C

7: Zn; AcOH / CH₂Cl₂ / 0.33 h / 20 °C

8: 451 mg / aq. HCl / tetrahydrofuran / 24 h / 20 °C

9: 91 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh / CH₂Cl₂ / 12 h / Heating

10: K₂CO₃ / methanol / 9 h / 0 °C

11: MnO₂ / CH₂Cl₂ / 72 h / 20 °C

12: aq. NaClO₂; KH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 3 h / 20 °C

13: 11 mg / SOCl₂ / 18 h / 20 °C

14: RuCl₃*3H₂O / 110 °C

15: CF₃CO₂H; BF₃*Et₂O / 0.17 h / 20 °C

16: 9 mg / TsOH / 40 h / 100 °C

With hydrogenchloride; manganese(IV) oxide; ruthenium trichloride; sodium chlorite; sodium periodate; potassium dihydrogenphosphate; Grubbs catalyst first generation; chloro-trimethyl-silane; thionyl chloride; 2-methyl-but-2-ene; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; boron trifluoride diethyl etherate; potassium carbonate; potassium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; triethylamine; trifluoroacetic acid; sodium iodide; zinc; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile; xylene; tert-butyl alcohol;
DOI:10.1016/j.tet.2004.07.040

Reference yield:

: 792948-20-0
(S)-4-vinyl-2,5-dihydropyrrole-1,2-dicarboxylic acid 2-methyl ester

: 792948-31-3
C₂₅H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 12 steps

1: TMSCl; NaI / acetonitrile / 10 h / 20 °C

2: 93 mg / Et₃N / CH₂Cl₂ / 12 h / 0 °C

3: Zn; AcOH / CH₂Cl₂ / 0.33 h / 20 °C

4: 451 mg / aq. HCl / tetrahydrofuran / 24 h / 20 °C

5: 91 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh / CH₂Cl₂ / 12 h / Heating

6: K₂CO₃ / methanol / 9 h / 0 °C

7: MnO₂ / CH₂Cl₂ / 72 h / 20 °C

8: aq. NaClO₂; KH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 3 h / 20 °C

9: 11 mg / SOCl₂ / 18 h / 20 °C

10: RuCl₃*3H₂O / 110 °C

11: CF₃CO₂H; BF₃*Et₂O / 0.17 h / 20 °C

12: 9 mg / TsOH / 40 h / 100 °C

With hydrogenchloride; manganese(IV) oxide; ruthenium trichloride; sodium chlorite; potassium dihydrogenphosphate; chloro-trimethyl-silane; thionyl chloride; 2-methyl-but-2-ene; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; acetic acid; triethylamine; trifluoroacetic acid; sodium iodide; zinc; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tet.2004.07.040