S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Base Information

Chemical Name:S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside
CAS No.:950761-43-0
Molecular Formula:C₃₀H₃₀O₄SSe
Molecular Weight:565.592
Hs Code.:

Synonyms:S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Suppliers and Price of S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

There total 5 articles about S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 950761-42-9
S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-β-D-thiogalactopyranoside

: 1666-13-3
diphenyl diselenide

: 950761-43-0
S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Guidance literature:: With tributylphosphine; In toluene; for 24h; Heating;
DOI:10.1021/jo070750s

Reference yield:

: 922182-99-8
S-phenyl 4,6-O-benzylidene-3-O-(2-naphthylmethyl)-β-D-thiogalactopyranoside

: 950761-43-0
S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaH / dimethylformamide; various solvent(s) / -15 - 20 °C

2: 95 percent / TsOH*H₂O / methanol / 0.75 h / Heating

3: 77 percent / Bu₃P / toluene / 24 h / Heating

With tributylphosphine; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo070750s

Reference yield:

: 950761-41-8
S-phenyl 4,6-O-benzylidene-2-O-methyl-3-O-(2-naphthylmethyl)-β-D-thiogalactopyranoside

: 950761-43-0
S-phenyl 2-O-methyl-3-O-(2-naphthylmethyl)-6-deoxy-6-phenylseleno-β-D-thiogalactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / TsOH*H₂O / methanol / 0.75 h / Heating

2: 77 percent / Bu₃P / toluene / 24 h / Heating

With tributylphosphine; toluene-4-sulfonic acid; In methanol; toluene;
DOI:10.1021/jo070750s