17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

Base Information

Chemical Name:17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene
CAS No.:88166-33-0
Molecular Formula:C₃₀H₃₇Cl₂NO₃
Molecular Weight:530.535
Hs Code.:

Synonyms:17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

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Chemical Property of 17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

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Technology Process of 17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

There total 3 articles about 17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 88166-29-4
3-benzyloxy-17β<-3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy> estra-1,3,5(10)triene

: 88166-33-0
17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; Ambient temperature; Heating;

Reference yield:

: 21447-59-6
3-N,N-bis(2-chloroethyl)amino-4-methyl-benzoyl-chloride

: 88166-33-0
17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / triethylamine / tetrahydrofuran / 3 h / Ambient temperature; Heating

2: 99 percent / H₂ / 5percent Pd/C / tetrahydrofuran; methanol / Ambient temperature; Heating

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;

Reference yield:

: 14982-15-1
3-benzyloxyestra-1,3,5(10)-trien-17β-ol

: 88166-33-0
17β<3'-N,N-bis(2''-chlorethyl)amino-4'-methyl-benzyloxy>-3-hydroxy-estra-1,3,5(10)triene

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / triethylamine / tetrahydrofuran / 3 h / Ambient temperature; Heating

2: 99 percent / H₂ / 5percent Pd/C / tetrahydrofuran; methanol / Ambient temperature; Heating

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;