bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

Base Information

Chemical Name:bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE
CAS No.:1269794-13-9
Molecular Formula:C₂₈H₃₃NO₁₄
Molecular Weight:607.568
Hs Code.:

Synonyms:bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

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Chemical Property of bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

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Technology Process of bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

There total 5 articles about bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23222-97-1
(2-nitro-1,4-phenylene)dimethanol

: 96297-73-3
methacrylic acid 2-(3-chlorocarbonylpropionyloxy)ethyl ester

: 1269794-13-9
bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c0sm00638f

Reference yield:

: 16255-50-8
1-nitro-2,5-bis-(chloromethyl)benzene

: 20882-04-6
2-methacryloyloxyethyl hydrogen succinate

: 1269794-13-9
bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

Guidance literature:: 2-methacryloyloxyethyl hydrogen succinate; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

1-nitro-2,5-bis-(chloromethyl)benzene; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5
2-methyl-2-propenoic acid 2-hydroxyethyl ester

: 1269794-13-9
bis(2-(methacryloyloxy)ethyl) O,O’-((2-nitro-1,4-phenylene)bis(methylene)) disuccinatE

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methoxy-phenol / neat (no solvent) / 18 h / 90 °C / Inert atmosphere; Sealed tube

2.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 18 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; potassium carbonate; 4-methoxy-phenol; In N,N-dimethyl-formamide;