(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

Base Information

Chemical Name:(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester
CAS No.:183665-60-3
Molecular Formula:C₂₂H₃₈N₂O₆
Molecular Weight:426.554
Hs Code.:

Synonyms:(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

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Chemical Property of (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

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Technology Process of (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

There total 1 articles about (R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21568-87-6
2-aminocaprolactam

: 183665-60-3
(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylsulfoxide

2: 1.) LiN(TMS)2 / 1.) THF, -78 deg C, 2.) THF

3: CF₃CO₂H

4: EDAC, HOBT

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hexamethyldisilazane; In dimethyl sulfoxide;
DOI:10.1016/S0960-894X(98)00370-9

Reference yield:

: 183665-60-3
(R)-3-((S)-1-Methoxycarbonylmethyl-2-oxo-azepan-3-ylcarbamoyl)-octanoic acid tert-butyl ester

: 183665-61-4
{(S)-3-[(R)-2-(Benzyloxycarbamoyl-methyl)-heptanoylamino]-2-oxo-azepan-1-yl}-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA

2: EDAC, HOBT

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
DOI:10.1016/S0960-894X(98)00370-9