C₅₉H₆₆Cl₄N₂O₁₄

Base Information

Chemical Name:C₅₉H₆₆Cl₄N₂O₁₄
CAS No.:1424402-40-3
Molecular Formula:C₅₉H₆₆Cl₄N₂O₁₄
Molecular Weight:1168.99
Hs Code.:

C<sub>59</sub>H<sub>66</sub>Cl<sub>4</sub>N<sub>2</sub>O<sub>14</sub>

Synonyms:C₅₉H₆₆Cl₄N₂O₁₄

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Chemical Property of C₅₉H₆₆Cl₄N₂O₁₄

Chemical Property:

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Technology Process of C₅₉H₆₆Cl₄N₂O₁₄

There total 14 articles about C₅₉H₆₆Cl₄N₂O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1424402-34-5
C₃₆H₄₅Cl₄NO₉

: 1424401-77-3
(S)-2-[(9H-fluorene-9-ylmethoxyarbonylamino)methyl]succinic acid 4-allyl ester

: 1424402-40-3
C₅₉H₆₆Cl₄N₂O₁₄

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm301346z

Reference yield:

: 1424401-73-9
4-((R)-4-benzyl-2-oxooxazolidine-3-yl)-4-butyric acid allyl ester

: 1424402-40-3
C₅₉H₆₆Cl₄N₂O₁₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / tetrahydrofuran; dichloromethane / 16 h / 20 °C / Inert atmosphere

3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: 16 h / Reflux; Inert atmosphere

5.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.67 h / 0 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere

7.1: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C / Inert atmosphere

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; lithium hydroxide monohydrate; dihydrogen peroxide; sodium hexamethyldisilazane; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jm301346z

Reference yield:

: 350245-09-9
2-(tert-butyl-dimethyl-silanyloxy)-4-methyl-pentanoyl chloride

: 1424402-40-3
C₅₉H₆₆Cl₄N₂O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice; Inert atmosphere

2: ammonium cerium (IV) nitrate / methanol / 17 h / 0 °C / Inert atmosphere

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; ammonium cerium (IV) nitrate; triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/jm301346z