Technology Process of C48H68O14Si
There total 26 articles about C48H68O14Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27H44BClO6Si; C29H32O9;
In
dichloromethane;
at -78 ℃;
for 4.25h;
Inert atmosphere;
With
diethyl methoxy borane;
In
tetrahydrofuran; methanol;
at -78 ℃;
for 0.416667h;
Further stages;
Inert atmosphere;
DOI:10.1021/ol301783p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 24 h / Inert atmosphere
2.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C / Inert atmosphere
3.1: dichloromethane / 4.25 h / -78 °C / Inert atmosphere
3.2: 0.42 h / -78 °C / Inert atmosphere
With
diisobutylaluminium hydride; potassium carbonate;
In
hexane; dichloromethane; acetone;
DOI:10.1021/ol301783p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 24 h / Inert atmosphere
2.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C / Inert atmosphere
3.1: dichloromethane / 4.25 h / -78 °C / Inert atmosphere
3.2: 0.42 h / -78 °C / Inert atmosphere
With
diisobutylaluminium hydride; potassium carbonate;
In
hexane; dichloromethane; acetone;
DOI:10.1021/ol301783p