4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

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Chemical Name:4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid
CAS No.:1334492-91-9
Molecular Formula:C₃₂H₃₃N₃O₆S
Molecular Weight:587.697
Hs Code.:

Synonyms:4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

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Chemical Property of 4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

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Technology Process of 4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

There total 11 articles about 4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1334492-91-9
4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; for 3h;

Reference yield:

: 1334493-50-3
C₃₉H₃₉N₃O₆S

: 1334492-91-9
4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

Guidance literature:: With trifluoroacetic acid; In toluene; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.06.056

Reference yield:

: 1334493-33-2
benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)benzoate

: 1334492-91-9
4-(N-(4-cyclohexylbenzyl)-2-(N-methylquinoline-8-sulfonamido)acetamido)-2-hydroxy-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / toluene / 0.08 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; trifluoroacetic acid; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.bmcl.2011.06.056