ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

Base Information

Chemical Name:ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate
CAS No.:140209-62-7
Molecular Formula:C₁₆H₂₄O₇
Molecular Weight:328.362
Hs Code.:

Synonyms:ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

Chemical Property:

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Technology Process of ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

There total 2 articles about ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 140225-28-1
Ethyl onate

: 140209-62-7
ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

: 140209-64-9
Ethyl onate

: 140209-63-8
Ethyl onate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In acetonitrile; at -25 ℃; for 0.0333333h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4020(01)88191-6

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 140209-55-8
Methyl 4:5,7:8-di-O-isopropylidene-2-thio-α-D-manno-octulopyranosonate

: 140209-62-7
ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

: 140209-64-9
Ethyl onate

: 140209-63-8
Ethyl onate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In acetonitrile; at -25 ℃; for 0.0333333h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4020(01)88191-6

Reference yield: 91.0%

: methyl 4-O-benzoyl-3-O-benzyl-α-L-rhamnopyranoside

: 140209-62-7
ethyl 2,6-anhydro-4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-oct-2-enosonate

: C₃₇H₄₇IO₁₃

Guidance literature:: With N-iodosaccharine; trifluorormethanesulfonic acid; In dichloromethane; toluene; acetonitrile; at 20 ℃; for 0.5h; Darkness; Inert atmosphere;