Technology Process of 4-fluoro-2-phenylphenol
There total 1 articles about 4-fluoro-2-phenylphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
ethanol;
for 2.5h;
Further byproducts given;
Ambient temperature;
Irradiation;
DOI:10.1021/jo9517196
- Guidance literature:
-
With
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; potassium carbonate;
In
1,4-dioxane;
at 120 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/chem.201706043
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aluminum (III) chloride / hexane / Inert atmosphere; Sealed tube; Reflux
2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / water; tetrahydrofuran / 24 h / 90 °C / Schlenk technique; Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; aluminum (III) chloride; potassium phosphate; palladium diacetate;
In
tetrahydrofuran; hexane; water;
DOI:10.1021/acs.joc.1c01770
