Technology Process of C23H26O3
There total 7 articles about C23H26O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 20 °C
2.1: potassium carbonate / methanol / 1 h / 20 °C
3.1: magnesium / tetrahydrofuran
3.2: 3 h / -40 °C
4.1: sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C
5.1: methanol; toluene-4-sulfonic acid / 24 h / 20 °C
6.1: triethylamine / dichloromethane / 1 h / 20 °C
7.1: potassium carbonate / methanol / 2 h / 20 °C
With
methanol; sodium hydride; di(n-butyl)tin oxide; potassium carbonate; toluene-4-sulfonic acid; magnesium; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.04.030
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C
2: methanol; toluene-4-sulfonic acid / 24 h / 20 °C
3: triethylamine / dichloromethane / 1 h / 20 °C
4: potassium carbonate / methanol / 2 h / 20 °C
With
methanol; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.04.030