7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

Base Information

Chemical Name:7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine
CAS No.:295780-93-7
Molecular Formula:C₁₇H₁₈N₂O₃
Molecular Weight:298.342
Hs Code.:

Synonyms:7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

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Technology Process of 7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

There total 3 articles about 7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 295780-91-5
5-[N'-(4-methoxybenzylidene)-N-methylhydrazino]-2,3-dimethyl-[1,4]benzoquinone

: 295780-93-7
7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

Guidance literature:: In methanol; for 0.166667h; Heating;
DOI:10.1016/S0040-4020(00)00185-X

Reference yield:

: 608-43-5
2,3-dimethyl-1,4-dihydroxybenzene

: 295780-93-7
7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / KBrO₃; H₂SO₄ / H₂O / 0.17 h / 80 °C

2: 39 percent / methanol / 0.08 h

3: 90 percent / methanol / 0.17 h / Heating

With potassium bromate; sulfuric acid; In methanol; water; 1: Oxidation / 2: Substitution / 3: Cyclization;
DOI:10.1016/S0040-4020(00)00185-X

Reference yield:

: 526-86-3
2,3-dimethyl-1,4-benzoquinone

: 295780-93-7
7-hydroxy-3-(4-methoxyphenyl)-1,5,6-trimethyl-1H-benzo[1,3,4]oxadiazine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / methanol / 0.08 h

2: 90 percent / methanol / 0.17 h / Heating

In methanol; 1: Substitution / 2: Cyclization;
DOI:10.1016/S0040-4020(00)00185-X