4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione

Base Information

• Chemical Name: 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione
• CAS No.: 195213-60-6
• Molecular Formula: C₂₀H₁₈ClNOS₂
• Molecular Weight: 387.954

Synonyms:4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione

Chemical Property of 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione

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Technology Process of 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione

There total 2 articles about 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

4-phenylpent-4-en-1-yl 4-methylbenzenesulfonate (182194-88-3) + N-(hydroxy)-4-(p-chlorophenyl)thiazole-2(3H)-thione tetraethylammonium salt → 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione (195213-60-6) + 4-(4-chloro-phenyl)-2-(4-phenyl-pent-4-enylsulfanyl)-thiazole 3-oxide

Guidance literature:

In N,N-dimethyl-formamide; at 25 ℃; Yields of byproduct given; dark;

DOI:10.1002/(SICI)1099-0690(199906)1999:6<1275::AID-EJOC1275>3.0.CO;2-2

Reference yield: 62.0%

4-phenylpent-4-en-1-yl 4-methylbenzenesulfonate (182194-88-3) + 4-(p-chlorophenyl)-N-hydroxythiazole-2(3H)-thione potassium salt → 4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione (195213-60-6)

Guidance literature:

In N,N-dimethyl-formamide; at 25 ℃;

DOI:10.1055/s-1997-5754

Reference yield: 60.0%

4-(4-chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione (195213-60-6) → 2-methyl-2-phenyltetrahydrofuran (2406-17-9,21865-78-1) + 3-phenyltetrahydro-2H-pyran (118408-32-5,16765-32-5) + 4-phenylpent-4-en-1-ol (93222-37-8)

Guidance literature:

With tri-n-butyl-tin hydride; at 20 ℃; Irradiation;

DOI:10.1055/s-1997-5754

upstream raw materials:

4-phenylpent-4-en-1-yl 4-methylbenzenesulfonate

Downstream raw materials:

2-methyl-2-phenyltetrahydrofuran

3-phenyltetrahydro-2H-pyran

4-phenylpent-4-en-1-ol

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