tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate

Base Information

• Chemical Name: tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate
• CAS No.: 1182206-79-6
• Molecular Formula: C₃₈H₄₁N₅O₉
• Molecular Weight: 711.772

Synonyms:tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate

Chemical Property of tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate

Chemical Property:

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Technology Process of tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate

There total 1 articles about tert-butyl N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-(2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazine)acetate (1182206-85-4) + C19H22BrN3O5 (1182206-88-7) → tert-butyl N4-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate (1182206-79-6)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

Reference yield: 82.0%

tert-butyl N4-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetate (1182206-79-6) → N4-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetic acid (1182206-89-8)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/hlca.200900047

upstream raw materials:

ethyl 2-(2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazine)acetate

C₁₉H₂₂BrN₃O₅

Downstream raw materials:

N₄-[(benzyloxy)carbonyl]-6-[(1-(2-ethoxy-2-oxoethyl)-2-{[(9H-fluoren-9-yl)methoxy]carbonyl}hydrazino)methyl]cytosine-1-acetic acid

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