phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine

Base Information

• Chemical Name: phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine
• CAS No.: 95970-27-7
• Molecular Formula: C₈H₅F₆NO₂S₂
• Molecular Weight: 325.256
• Mol file: 95970-27-7.mol

Synonyms:phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine

Chemical Property of phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine

There total 3 articles about phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N-dichlorotrifluoromethylsulfonamide (54285-45-9) + phenyl trifluoromethylsulfide (456-56-4) → phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine (95970-27-7)

Guidance literature:

for 48h;

Reference yield: 84.0%

trifluoromethylsulfonic anhydride (358-23-6) + phenyl trifluoromethyl sulfilimine (1260111-65-6) → phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine (95970-27-7)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/adsc.201000494

Reference yield: 70.0%

Trifluoromethanesulfonamide (421-85-2) + phenyl trifluoromethyl sulfoxide (703-18-4) → phenyl N-(trifluoromethanesulfonyl) trifluoromethyl sulfilimine (95970-27-7)

Guidance literature:

With trifluoromethanesulfonic acid anhydride; for 12h; 1.) 40 deg C, 10 min, 2.) 20 deg C, 12 h;;

upstream raw materials:

Trifluoromethanesulfonamide

phenyl trifluoromethyl sulfoxide

N,N-dichlorotrifluoromethylsulfonamide

phenyl trifluoromethylsulfide