methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Base Information

• Chemical Name: methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate
• CAS No.: 1022160-16-2
• Molecular Formula: C₄₄H₅₂N₄O₉
• Molecular Weight: 780.918

Synonyms:methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Chemical Property of methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Chemical Property:

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Technology Process of methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

There total 1 articles about methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1) + glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) → methyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-16-2)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 97.0%

methyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-16-2) → N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

glycine ethyl ester hydrochloride

Downstream raw materials:

N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

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