C₃₆H₆₂O₆Si₂

Base Information

Chemical Name:C₃₆H₆₂O₆Si₂
CAS No.:934560-30-2
Molecular Formula:C₃₆H₆₂O₆Si₂
Molecular Weight:647.056
Hs Code.:

C<sub>36</sub>H<sub>62</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₆H₆₂O₆Si₂

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Chemical Property of C₃₆H₆₂O₆Si₂

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Technology Process of C₃₆H₆₂O₆Si₂

There total 8 articles about C₃₆H₆₂O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 934560-36-8
C₃₀H₄₈O₆Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 934560-30-2
C₃₆H₆₂O₆Si₂

Guidance literature:: With 2,6-dimethylpyridine; triethylamine; at 0 ℃; for 0.5h;
DOI:10.1039/b616558c

Reference yield:

: 863659-96-5
2-Methyl-2-[(2R,6S)-6-(2-oxo-ethyl)-tetrahydro-pyran-2-yl]-propionic acid methyl ester

: 934560-30-2
C₃₆H₆₂O₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: (+)-DIPBr / tetrahydrofuran / -78 °C

2.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

3.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

4.1: osmium tetraoxide; NMO / 12 h

4.2: 90 percent / NaIO₄ / 0.5 h

5.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

6.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

7.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; sodium hydride; triethylamine; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Brown allylation / 5.1: Brown crotylation;
DOI:10.1039/b616558c

Reference yield:

: C₁₉H₂₇O₄Br

: 934560-30-2
C₃₆H₆₂O₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: H₂; NaHCO₃ / Pd/C / 24 h

1.2: Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 0 °C

2.1: (+)-DIPBr / tetrahydrofuran / -78 °C

3.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

4.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

5.1: osmium tetraoxide; NMO / 12 h

5.2: 90 percent / NaIO₄ / 0.5 h

6.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

7.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

8.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; hydrogen; sodium hydride; sodium hydrogencarbonate; triethylamine; palladium on activated charcoal; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.2: Dess-Martin oxidation / 2.1: Brown allylation / 6.1: Brown crotylation;
DOI:10.1039/b616558c