trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Base Information

Chemical Name:trans-3-Methyl-5-phenyl-1-methylidenecyclohexane
CAS No.:28467-40-5
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

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Technology Process of trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

There total 19 articles about trans-3-Methyl-5-phenyl-1-methylidenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7214-50-8
5-methylcyclohex-2-en-1-one

: 591-51-5
phenyllithium

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With copper(I) thiocyanate; In diethyl ether; at -78 ℃; for 1h; Mechanism; Product distribution; other reagents: CuI;
DOI:10.1021/jo00152a026

Reference yield:

: 7214-50-8
5-methylcyclohex-2-en-1-one

: 28557-00-8
phenylzinc chloride

: 28467-39-2,28467-40-5,60741-75-5
cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol300387f

Reference yield:

: 7214-50-8
5-methylcyclohex-2-en-1-one

: 28557-00-8
phenylzinc chloride

: 28467-39-2,28467-40-5,60741-75-5
cis-3-Methyl-5-phenyl-1-methylidenecyclohexane

: 28467-40-5
trans-3-Methyl-5-phenyl-1-methylidenecyclohexane

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol300387f