C₂₄H₂₂F₂N₂O₄

Base Information

Chemical Name:C₂₄H₂₂F₂N₂O₄
CAS No.:1363375-17-0
Molecular Formula:C₂₄H₂₂F₂N₂O₄
Molecular Weight:440.446
Hs Code.:

C<sub>24</sub>H<sub>22</sub>F<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₂F₂N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₂F₂N₂O₄

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Technology Process of C₂₄H₂₂F₂N₂O₄

There total 7 articles about C₂₄H₂₂F₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₁₂F₂N₂O₂*2ClH

: C₂₄H₁₁F₅O₃

: 1363375-17-0
C₂₄H₂₂F₂N₂O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;

Reference yield:

: C₂₂H₂₄F₂N₂O₆S

: 1363375-17-0
C₂₄H₂₂F₂N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sodium iodide; trifluoroacetic anhydride / acetone / 0.63 h / 0 °C / Inert atmosphere

2: hydrogenchloride / methanol / 18 h / 20 °C

3: triethylamine / tetrahydrofuran / 14.5 h / 0 - 20 °C

4: water; sodium phosphinate hydrate / Raney Ni / methanol / 3 h / 20 °C / pH 5.2 / Inert atmosphere; Aqueous acetate buffer

5: hydrogenchloride / 1,4-dioxane / 14 h / 20 °C

6: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

With hydrogenchloride; sodium phosphinate hydrate; water; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; sodium iodide; Raney Ni; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: C₂₂H₂₂F₂N₂O₅S

: 1363375-17-0
C₂₄H₂₂F₂N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: water; aluminum oxide / chloroform / 72 h / 20 °C / Inert atmosphere

2: sodium iodide; trifluoroacetic anhydride / acetone / 0.63 h / 0 °C / Inert atmosphere

3: hydrogenchloride / methanol / 18 h / 20 °C

4: triethylamine / tetrahydrofuran / 14.5 h / 0 - 20 °C

5: water; sodium phosphinate hydrate / Raney Ni / methanol / 3 h / 20 °C / pH 5.2 / Inert atmosphere; Aqueous acetate buffer

6: hydrogenchloride / 1,4-dioxane / 14 h / 20 °C

7: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

With hydrogenchloride; aluminum oxide; sodium phosphinate hydrate; water; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; sodium iodide; Raney Ni; In tetrahydrofuran; 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide; acetone;