C₅₅H₃₉BrN₆NiO

Base Information

• Chemical Name: C₅₅H₃₉BrN₆NiO
• CAS No.: 1398163-08-0
• Molecular Formula: C₅₅H₃₉BrN₆NiO
• Molecular Weight: 938.548
• Mol file: 1398163-08-0.mol

Synonyms:C₅₅H₃₉BrN₆NiO

Chemical Property of C₅₅H₃₉BrN₆NiO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₅₅H₃₉BrN₆NiO

There total 1 articles about C₅₅H₃₉BrN₆NiO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

(2-amino-5,10,15,20-tetraphenylporphyrinato)-nickel(II) (189192-29-8) + 5,7-dibromo-1,3,3-trimethylindolin-2-one → C55H39BrN6NiO (1398163-08-0) + C99H67N11Ni2O (1398163-13-7)

Guidance literature:

With potassium tert-butylate; palladium diacetate; XPhos; In toluene; at 100 - 110 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

DOI:10.1016/j.tet.2012.07.024

Reference yield: 42.0%

(2-amino-5,10,15,20-tetraphenylporphyrinato)-nickel(II) (189192-29-8) + C55H39BrN6NiO (1398163-08-0) → C99H67N11Ni2O (1398163-13-7)

Guidance literature:

With potassium tert-butylate; palladium diacetate; XPhos; In toluene; at 100 - 110 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2012.07.024

upstream raw materials:

(2-amino-5,10,15,20-tetraphenylporphyrinato)-nickel(II)

Downstream raw materials:

C₉₉H₆₇N₁₁Ni₂O