2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide

Base Information

• Chemical Name: 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide
• CAS No.: 478399-10-9
• Molecular Formula: C₁₇H₂₁Cl₂NO₅S
• Molecular Weight: 422.329

Synonyms:2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide

Chemical Property of 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide

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Technology Process of 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide

There total 4 articles about 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(2,5-dichloro-4-isopropyloxyphenyl)-4,5,6,7-tetrahydro-4H-cyclohepta[d]-benzisothiazolium perchlorate → 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide (478399-10-9)

Guidance literature:

With 30percent H₂O₂; In acetic acid; at 45 ℃; for 4h;

DOI:10.1021/jo0202841

Reference yield:

2-chlorocyclohept-1-ene-1-carbaldehyde (1633-67-6) → 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide (478399-10-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 2 h / 20 °C

2: 88 percent / HClO₄ / 1 h / 20 °C

3: 80 percent / 30percent H₂O₂ / acetic acid / 4 h / 45 °C

With perchloric acid; In acetic acid;

DOI:10.1021/jo0202841

Reference yield:

2-thiocyanatocyclohept-1-enecarbaldehyde (42141-26-4) → 2-(2,5-dichloro-4-isopropyloxyphenyl)-3-hydroperoxy-2,3,5,6,7,8-hexahydro-4H-cyclohepta[d]isothiazole 1,1-dioxide (478399-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / HClO₄ / 1 h / 20 °C

2: 80 percent / 30percent H₂O₂ / acetic acid / 4 h / 45 °C

With perchloric acid; In acetic acid;

DOI:10.1021/jo0202841

upstream raw materials:

2-chlorocyclohept-1-ene-1-carbaldehyde

2-thiocyanatocyclohept-1-enecarbaldehyde

cycloheptanone

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