[3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester

Base Information

• Chemical Name: [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester
• CAS No.: 942399-54-4
• Molecular Formula: C₁₉H₂₈F₃NO₅
• Molecular Weight: 407.43

Synonyms:[3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester

Chemical Property of [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester

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Technology Process of [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester

There total 1 articles about [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-(4-benzyloxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]allylcarbamic acid t-butyl ester (942399-55-5) → [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester (942399-54-4)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; at 20 ℃; for 24h;

Reference yield:

1-Bromoheptane (629-04-9) + [3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester (942399-54-4) → [3-(4-heptyloxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester (942399-56-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 6h;

Reference yield:

[3-(4-hydroxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester (942399-54-4) + 1-bromo-3-[4-(trifluoromethyl)phenyl]propane (178369-93-2) → (1-(methoxymethoxy)methyl-1-methyl-3-{3-trifluoromethyl-4-[3-(4-trifluoromethylphenyl)propoxy]phenyl})propylcarbamic acid t-butyl ester (1093172-58-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1.5h;

upstream raw materials:

[3-(4-benzyloxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]allylcarbamic acid t-butyl ester

Downstream raw materials:

[3-(4-heptyloxy-3-trifluoromethylphenyl)-1-(methoxymethoxy)methyl-1-methyl]propylcarbamic acid t-butyl ester

(1-(methoxymethoxy)methyl-1-methyl-3-{3-trifluoromethyl-4-[3-(4-trifluoromethylphenyl)propoxy]phenyl})propylcarbamic acid t-butyl ester

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