(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

Base Information

Chemical Name:(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide
CAS No.:250788-95-5
Molecular Formula:C₂₁H₂₁Cl₂N₅O₂
Molecular Weight:446.336
Hs Code.:

Synonyms:(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

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Chemical Property of (S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

Chemical Property:

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Technology Process of (S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

There total 15 articles about (S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 191604-61-2
2-methoxy-5-(1H-tetrazol-1-yl)benzoyl chloride

: 156300-01-5,206997-68-4
(S)-N-methyl-(2-(3,4-dichlorophenyl)pent-4-enyl)amine

: 250788-95-5
(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; for 18h;

Reference yield:

: 96-97-9
5-nitrosalicylic acid

: 250788-95-5
(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetone / 74 h / Heating / reflux

2.1: hydrogen / 5%-palladium/activated carbon / methanol / 17 h / 2585.81 Torr

3.1: orthoformic acid triethyl ester / acetic acid / 20 h

3.2: 1 h / 70 °C

4.1: sodium hydroxide; water / methanol / 4 h / Heating / reflux

5.1: oxalyl dichloride / DMF (N,N-dimethyl-formamide); dichloromethane / 4 h

6.1: sodium hydrogencarbonate / water; acetone / 18 h

With sodium hydroxide; oxalyl dichloride; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; orthoformic acid triethyl ester; 5%-palladium/activated carbon; In methanol; DMF (N,N-dimethyl-formamide); dichloromethane; water; acetic acid; acetone;

Reference yield:

: 34841-11-7
methyl 2-methoxy-5-nitrobenzoate

: 250788-95-5
(S)-N-methyl-N-(2-(3,4-dichlorophenyl)pent-4-enyl)-2-methoxy-5-(1H-tetrazol-1-yl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / 5%-palladium/activated carbon / methanol / 17 h / 2585.81 Torr

2.1: orthoformic acid triethyl ester / acetic acid / 20 h

2.2: 1 h / 70 °C

3.1: sodium hydroxide; water / methanol / 4 h / Heating / reflux

4.1: oxalyl dichloride / DMF (N,N-dimethyl-formamide); dichloromethane / 4 h

5.1: sodium hydrogencarbonate / water; acetone / 18 h

With sodium hydroxide; oxalyl dichloride; water; hydrogen; sodium hydrogencarbonate; orthoformic acid triethyl ester; 5%-palladium/activated carbon; In methanol; DMF (N,N-dimethyl-formamide); dichloromethane; water; acetic acid; acetone;