5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

Base Information

Chemical Name:5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde
CAS No.:1146433-79-5
Molecular Formula:C₃₉H₄₃NO₃S₂
Molecular Weight:637.907
Hs Code.:

Synonyms:5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

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Chemical Property of 5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

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Technology Process of 5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

There total 3 articles about 5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1146433-78-4
N-(4-(5-bromothiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine

: (5-formylthiophen-2-yl)boronic acid

: 1146433-79-5
5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In methanol; toluene; at 75 ℃; for 0.25h; Microwave irradiation;
DOI:10.1002/anie.200804719

Reference yield:

: 1040281-83-1
5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophene-2-carboxaldehyde

: 1146433-78-4
N-(4-(5-bromothiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine

: 1146433-79-5
5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/co500071x

Reference yield:

: 1380786-94-6
(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)boronic acid

: 1146433-79-5
5-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)thiophene-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium carbonate / tetrahydrofuran; water / Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; 1: |Suzuki-Miyaura Coupling / 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/co500071x