N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide)

Base Information

• Chemical Name: N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide)
• CAS No.: 464885-21-0
• Molecular Formula: C₁₂₄H₁₂₈Br₂N₂O₈
• Molecular Weight: 1934.2
• Mol file: 464885-21-0.mol

Synonyms:N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide)

Chemical Property of N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide)

There total 1 articles about N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8⁽⁹⁾,18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N,N’-bis-(N-2,6-diisopropylphenyl)-1,6,8(9),11,16,18-hexabromoquaterrylene-3,4:13,14-bis(dicarboximide) (464885-17-4) + tert-octylphenol (140-66-9) → N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8(9),18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide) (464885-21-0)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 110 ℃; for 48h;

DOI:10.1002/chem.200700523

Reference yield: 46.0%

N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8(9),18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide) (464885-21-0) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8,9:18,19-dinaphthoquaterrylene-3,4:13,14-bis(dicarboximide)

Guidance literature:

With cesium fluoride; tris-(o-tolyl)phosphine; [Pd(dibenzylideneacetone)2]; In toluene; acetonitrile; at 95 ℃; for 48h;

DOI:10.1002/chem.200700523

Reference yield:

piperidine (110-89-4) + N,N'-bis(N-2,6-diisopropylphenyl)-1,6,11,16-tetrakis[4-(1,1,3,3-tetramethylbutyl)phenoxy]-8(9),18-dibromoquaterrylene-3,4:13,14-bis(dicarboximide) (464885-21-0) + N,N'-(2,6-diisopropylphenyl)-1,6,11,16-tetra(4-tert-octylphenoxy)-8,19-dibromoquaterrylene-3,4:13,14-tetracarboxylic acid diimide → N,N'-(2,6-diisopropylphenyl)-1,6,11,16-tetra(4-tert-octylphenoxy)-8,19-di(N-piperidyl)quaterrylene-3,4:13,14-tetracarboxylic acid diimide + N,N'-(2,6-diisopropylphenyl)-1,6,11,16-tetra(4-tert-octylphenoxy)-8,18-di(N-piperidyl)quaterrylene-3,4:13,14-tetracarboxylic acid diimide

Guidance literature:

at 85 ℃; for 120h;

upstream raw materials:

N,N’-bis-(N-2,6-diisopropylphenyl)-1,6,8(9),11,16,18-hexabromoquaterrylene-3,4:13,14-bis(dicarboximide)

tert-octylphenol