C₁₇H₂₇BO₂

Base Information

Chemical Name:C₁₇H₂₇BO₂
CAS No.:177950-00-4
Molecular Formula:C₁₇H₂₇BO₂
Molecular Weight:274.211
Hs Code.:

C<sub>17</sub>H<sub>27</sub>BO<sub>2</sub>

Synonyms:C₁₇H₂₇BO₂

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Chemical Property of C₁₇H₂₇BO₂

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Technology Process of C₁₇H₂₇BO₂

There total 6 articles about C₁₇H₂₇BO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 74-97-5
chlorobromomethane

: 1438827-34-9
4,4,5,5-tetramethyl-2-(1-phenylbutyl)-1,3,2-dioxaborolane

: 177950-00-4
C₁₇H₂₇BO₂

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 2.08h; Inert atmosphere;
DOI:10.1021/ja403462b

Reference yield:

: 71813-50-8
1-bromo-2-(but-3-enyl)benzene

: 177950-00-4
C₁₇H₂₇BO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2-Nitrobenzenesulfonyl chloride; hydrazine hydrate / acetonitrile / 18 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

3.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Glovebox

4.1: chloro-trimethyl-silane; potassium iodide; water / acetonitrile / 2 h / 25 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -78 - 25 °C / Inert atmosphere

With n-butyllithium; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; water; hydrazine hydrate; 2-Nitrobenzenesulfonyl chloride; potassium iodide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/ja403462b

Reference yield:

: 13397-98-3
1-bromo-2-butylbenzene

: 177950-00-4
C₁₇H₂₇BO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

2.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Glovebox

3.1: chloro-trimethyl-silane; potassium iodide; water / acetonitrile / 2 h / 25 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -78 - 25 °C / Inert atmosphere

With n-butyllithium; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; water; potassium iodide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/ja403462b