dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

Base Information

Chemical Name:dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate
CAS No.:868599-64-8
Molecular Formula:C₃₄H₅₆N₆O₄
Molecular Weight:612.856
Hs Code.:

Synonyms:dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

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Chemical Property of dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

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Technology Process of dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

There total 1 articles about dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 28691-27-2
methyl 11-aminoundecanoate

: 30369-82-5
benzyl-(4,6-dichloro-[1,3,5]triazin-2-yl)amine

: 868599-64-8
dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 24h; Heating;
DOI:10.1021/jm050234z

Reference yield:

: 868599-64-8
dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

: 868599-65-9
11-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; for 1h; Heating;
DOI:10.1021/jm050234z

Reference yield:

: 868599-64-8
dimethyl 11,11'-{[6-(benzylamino)-1,3,5-triazine-2,4-diyl]diimino}diundecanoate

: C₆₂H₉₂Cl₂N₁₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / dioxane; H₂O / 1 h / Heating

2: 43 percent / HOBt; EDC; Et₃N / CH₂Cl₂ / 24 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jm050234z