Technology Process of C39H58N6O9
There total 8 articles about C39H58N6O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 50 percent / EtOCOCl; Et3N / tetrahydrofuran / -5 °C
2: 95 percent / Dess-Martin periodinane / CH2Cl2
With
chloroformic acid ethyl ester; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; dichloromethane;
2: Dess-Martin oxidation;
DOI:10.1016/j.bmcl.2005.12.013
- Guidance literature:
-
Multi-step reaction with 6 steps
1: CH2Cl2
2: 77 percent / aq. LiOH / tetrahydrofuran
3: 90 percent / HATU; DIPEA / dimethylformamide / -20 °C
4: 100 percent / HCl / dioxane
5: 50 percent / EtOCOCl; Et3N / tetrahydrofuran / -5 °C
6: 95 percent / Dess-Martin periodinane / CH2Cl2
With
hydrogenchloride; lithium hydroxide; chloroformic acid ethyl ester; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
1: Passerini reaction / 6: Dess-Martin oxidation;
DOI:10.1016/j.bmcl.2005.12.013