(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide

Base Information

• Chemical Name: (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide
• CAS No.: 1019970-94-5
• Molecular Formula: C₂₇H₃₇F₈N₃O₂S
• Molecular Weight: 619.663

Synonyms:(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide

Chemical Property of (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide

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Technology Process of (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide

There total 1 articles about (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-methyloxirane-2-carboxamide (512776-95-3) + N-methyl-9-(4,4,5,5,5-pentafluoropentylthio)nonan-1-amine hydrochloride (1019975-43-9) → (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide (1019970-94-5)

Guidance literature:

With diisopropylamine; In ipa; at 130 ℃; for 0.25h; Microwave irradiation;

Reference yield: 24.0%

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide (1019970-94-5) → (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylsulfinyl)nonyl]amino]propanamide (1019971-01-7)

Guidance literature:

With ammonium cerium(IV) nitrate; silica gel; In dichloromethane; water; at 20 ℃; for 1h;

Reference yield: 15.0%

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylthio)nonyl]amino]propanamide (1019970-94-5) → (2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylsulfonyl)nonyl]amino]propanamide (1019971-09-5)

Guidance literature:

With tetra-butylammonium hydrogen monopersulfate; In dichloromethane; at 20 ℃; for 2.5h;

upstream raw materials:

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-methyloxirane-2-carboxamide

N-methyl-9-(4,4,5,5,5-pentafluoropentylthio)nonan-1-amine hydrochloride

Downstream raw materials:

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylsulfinyl)nonyl]amino]propanamide

(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methyl-3-[N-methyl-N-[9-(4,4,5,5,5-pentafluoropentylsulfonyl)nonyl]amino]propanamide

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