3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

Base Information

Chemical Name:3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol
CAS No.:1307809-94-4
Molecular Formula:C₂₅H₂₇NO₃
Molecular Weight:389.494
Hs Code.:

Synonyms:3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

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Chemical Property of 3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

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Technology Process of 3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

There total 3 articles about 3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1307815-56-0
C₂₆H₂₉NO₃

: 1307809-94-4
3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

Guidance literature:: C₂₆H₂₉NO₃; With boron tribromide; In dichloromethane; at 0 ℃; for 5h;

With methanol; In dichloromethane;

Reference yield:

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 1307809-94-4
3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; sodium acetate / methanol / 2 h / 80 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / 0 - 20 °C

2.2: 0.67 h / 20 °C

2.3: 1 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 5 h / 0 °C

With n-butyllithium; hydroxylamine hydrochloride; sodium acetate; boron tribromide; In tetrahydrofuran; methanol; hexane; dichloromethane;

Reference yield:

: 54951-36-9
6-methoxy-1-tetralone oxime

: 1307809-94-4
3-(2-(1-(4-hydroxyphenyl)cyclohexyl)ethyl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / 0 - 20 °C

1.2: 0.67 h / 20 °C

1.3: 1 h / 0 - 20 °C

2.1: boron tribromide / dichloromethane / 5 h / 0 °C

With n-butyllithium; boron tribromide; In tetrahydrofuran; hexane; dichloromethane;