C₂₆H₃₂N₂O₇S

Base Information

Chemical Name:C₂₆H₃₂N₂O₇S
CAS No.:141321-41-7
Molecular Formula:C₂₆H₃₂N₂O₇S
Molecular Weight:516.615
Hs Code.:

C<sub>26</sub>H<sub>32</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₆H₃₂N₂O₇S

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Chemical Property of C₂₆H₃₂N₂O₇S

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Technology Process of C₂₆H₃₂N₂O₇S

There total 5 articles about C₂₆H₃₂N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: C₂₆H₃₀N₂O₇S

: 141321-41-7
C₂₆H₃₂N₂O₇S

Guidance literature:: With lithium borohydride; In tetrahydrofuran; for 16h; Heating;
DOI:10.1021/ja00071a025

Reference yield:

: 141321-39-3
C₂₆H₂₈N₂O₅S

: 141321-41-7
C₂₆H₃₂N₂O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / N-methylmorpholine N-oxide, osmium tetroxide / 2-methyl-propan-2-ol; tetrahydrofuran; H₂O / 2 h / 25 °C

2: 56 percent / lithium borohydride / tetrahydrofuran / 16 h / Heating

With osmium(VIII) oxide; lithium borohydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1021/ja00071a025

Reference yield:

: 141321-46-2
(E)-6β-(hydroxymethyl)-12-(2-hydroxyethylidene)-7-((4-methoxyphenyl)sulfonyl)-1,2,3aβ,4,5β,6,6a,7-octahydro-3,5-ethano-3H-pyrrolo<2,3-d>carbazole

: 141321-41-7
C₂₆H₃₂N₂O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / DBU / CH₂Cl₂ / -20 °C

2: 70 percent / SO₃*pyridine, triethylamine, DMSO / 4 h / 25 °C

3: 60 percent / pyridine*HF/pyridine / 2 h / 0 °C

4: 72 percent / N-methylmorpholine N-oxide, osmium tetroxide / 2-methyl-propan-2-ol; tetrahydrofuran; H₂O / 2 h / 25 °C

5: 56 percent / lithium borohydride / tetrahydrofuran / 16 h / Heating

With pyridine; osmium(VIII) oxide; lithium borohydride; pyridine-SO₃ complex; pyridine hydrogenfluoride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja00071a025