2-Nitrotetrafluorbenzonitril

Base Information

Chemical Name:2-Nitrotetrafluorbenzonitril
CAS No.:16583-05-4
Molecular Formula:C₇F₄N₂O₂
Molecular Weight:220.083
Hs Code.:

Synonyms:2-Nitrotetrafluorbenzonitril

Suppliers and Price of 2-Nitrotetrafluorbenzonitril

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Nitrotetrafluorbenzonitril

Chemical Property:

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Technology Process of 2-Nitrotetrafluorbenzonitril

There total 8 articles about 2-Nitrotetrafluorbenzonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 16582-99-3
2-NH₂-C₆F₄CN

: 407-25-0
trifluoroacetic anhydride

: 16583-05-4
2-Nitrotetrafluorbenzonitril

Guidance literature:: With dihydrogen peroxide; In dichloromethane; oxidation at 0°C 1.33 h (with 85% H2O2); heating in reflux 5 h;
DOI:10.1016/S0040-4020(01)92570-0

Reference yield:

: 5580-79-0
2,3,4,5-tetrafluoro-1-nitrobenzene

: 16583-05-4
2-Nitrotetrafluorbenzonitril

Guidance literature:: Multi-step reaction with 5 steps

1: Sn, aq. HCl

2: Br₂ / Heating

3: aq. H₂SO₄ / Heating

4: dimethylformamide / Heating

5: aq. H₂O₂, (CF₃CO)2O / CH₂Cl₂ / Heating

With hydrogenchloride; tin; sulfuric acid; dihydrogen peroxide; bromine; trifluoroacetic anhydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)92570-0