2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate

Base Information

• Chemical Name: 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate
• CAS No.: 1253186-02-5
• Molecular Formula: C₈₉H₇₈Cl₃NO₂₆
• Molecular Weight: 1683.95

Synonyms:2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate

Chemical Property of 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate

There total 1 articles about 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C87H78O26 + trichloroacetonitrile (545-06-2) → 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate (1253186-02-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1016/j.carres.2010.07.023

Reference yield: 79.0%

p-methoxylphenyl 2,4-di-O-benzoyl-α-L-6-deoxytalopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranoside (1253185-96-4) + 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl trichloroacetimidate (1253186-02-5) → p-methoxylphenyl 2,3,4-tri-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-6-deoxy-talopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 - 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

DOI:10.1016/j.carres.2010.07.023

upstream raw materials:

trichloroacetonitrile

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