1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

Base Information

Chemical Name:1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester
CAS No.:900183-71-3
Molecular Formula:C₃₁H₃₁NO₄
Molecular Weight:481.591
Hs Code.:

Synonyms:1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

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Chemical Property of 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

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Technology Process of 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

There total 1 articles about 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 35120-18-4
ethyl 1-bromocyclobutane-1-carboxylate

: 900183-71-3
1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

Guidance literature:: {1-[4-(hydroxymethyl)phenyl]-2-methyl-1H-indole-3-yl}(4-methylphenyl)methanone; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

ethyl 1-bromocyclobutane-1-carboxylate; In tetrahydrofuran; at 60 ℃; for 6h;

Reference yield: 43.0%

: 900183-71-3
1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

aqueous potassium hydrogen sulfate: aqueous potassium hydrogen sulfate

: 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol;

Reference yield: 43.0%

: 900183-71-3
1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester

: 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid

Guidance literature:: 1-({4-[2-methyl-3-(4-methylbenzoyl)-1H-indole-1-yl]benzyl}oxy)cyclobutanecarboxylic acid ethyl ester; With sodium hydroxide; water; In tetrahydrofuran; methanol; for 20h;

With potassium hydrogensulfate; In tetrahydrofuran; methanol; water; pH=4;