4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane

Base Information

• Chemical Name: 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane
• CAS No.: 26237-86-5
• Molecular Formula: C₂₉H₃₂N₂O₃
• Molecular Weight: 456.585

Synonyms:4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane

Chemical Property of 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane

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Technology Process of 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane

There total 3 articles about 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5α-epoxy-3,6-dimethoxy-N-methyl-2'-phenyl-6α,14α-endo-ethenopyrrolo<3,4-i>isomorphinane-1',3'-dione (26237-85-4) → 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane (26237-86-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1039/j39700000560

Reference yield:

N-phenyl-maleimide (941-69-5) → 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane (26237-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; In tetrahydrofuran; benzene;

DOI:10.1039/j39700000560

Reference yield:

thebaine (115-37-7) → 4,5α-epoxy-3,6-dimethoxy-17-methyl-1'-phenyl-(7β,8β)-8,1',2',5'-tetrahydro-7H-6α,14α-etheno-pyrrolo[3',4':7,8]morphinane (26237-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; In tetrahydrofuran; benzene;

DOI:10.1039/j39700000560

upstream raw materials:

4,5α-epoxy-3,6-dimethoxy-N-methyl-2'-phenyl-6α,14α-endo-ethenopyrrolo<3,4-i>isomorphinane-1',3'-dione

N-phenyl-maleimide

thebaine

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