(+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine

Base Information

• Chemical Name: (+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine
• CAS No.: 1160714-36-2
• Molecular Formula: C₃₁H₄₇N₃O₄Si₂
• Molecular Weight: 581.903

Synonyms:(+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine

Chemical Property of (+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine

Chemical Property:

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Technology Process of (+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine

There total 1 articles about (+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

4-N-benzoylcytosine (26661-13-2) + (+/-)-4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enol (1160714-21-5) → (+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N(4)-benzoylcytosine (1160714-36-2)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; N,N-dimethyl-formamide; at -20 ℃;

DOI:10.1080/15257770802458246

Reference yield: 71.0%

(+/-)-1-[4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enyl]-N(4)-benzoylcytosine (1160714-36-2) → (+/-)-1-[4,4-bis(hydroxymethyl)-5-methylenecyclopent-2-enyl]-N(4)-benzoylcytosine (1160714-37-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetonitrile; at 20 ℃;

DOI:10.1080/15257770802458246

upstream raw materials:

4-N-benzoylcytosine

(+/-)-4,4-bis(tert-butyldimethylsilanyloxymethyl)-5-methylenecyclopent-2-enol

Downstream raw materials:

(+/-)-1-[4,4-bis(hydroxymethyl)-5-methylenecyclopent-2-enyl]-N⁽⁴⁾-benzoylcytosine

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