4-amino-2-(morpholin-4-ylmethyl)phenol

Base Information

• Chemical Name: 4-amino-2-(morpholin-4-ylmethyl)phenol
• CAS No.: 6969-62-6
• Molecular Formula: C11H16 N2 O2 . 2 Cl H
• Molecular Weight: 208.2569

Synonyms:Phenol,4-amino-2-(4-morpholinylmethyl)-, dihydrochloride (9CI); o-Cresol, 4-amino-a-morpholino-, dihydrochloride(5CI)

Chemical Property of 4-amino-2-(morpholin-4-ylmethyl)phenol

Chemical Property:

• Vapor Pressure: 1.93E-06mmHg at 25°C
• Boiling Point: 383.9°Cat760mmHg
• Flash Point: 186°C
• Density: 1.242g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-amino-2-(morpholin-4-ylmethyl)phenol

There total 2 articles about 4-amino-2-(morpholin-4-ylmethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4-acetamido-α-(N-morpholino)-o-cresol (13886-00-5) → 4-amino-2-morpholinomethyl-phenol; dihydrochloride (6969-62-6)

Guidance literature:

With hydrogenchloride; for 5h; Reflux;

DOI:10.1016/j.ejmech.2018.08.016

Reference yield:

4-acetaminophenol (103-90-2,8055-08-1) → 4-amino-2-morpholinomethyl-phenol; dihydrochloride (6969-62-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 90 °C

2: hydrogenchloride / 5 h / Reflux

With hydrogenchloride; In ethanol;

DOI:10.1016/j.ejmech.2018.08.016

Reference yield: 82.0%

2-Methyl-5,6,7,8-tetrahydro-4H-<1>benzothieno<2,3-d><1,3>oxazin-4-on (13130-47-7) + 4-amino-2-morpholinomethyl-phenol; dihydrochloride (6969-62-6) → 3-(4-Hydroxy-3-morpholin-4-ylmethyl-phenyl)-2-methyl-5,6,7,8-tetrahydro-3H-benzo[4,5]thieno[2,3-d]pyrimidin-4-one (76226-56-7)

Guidance literature:

With sodium acetate; In acetic acid; for 3h; Heating;

upstream raw materials:

4-acetamido-α-(N-morpholino)-o-cresol

4-acetaminophenol

Downstream raw materials:

3-(4-Hydroxy-3-morpholin-4-ylmethyl-phenyl)-2-methyl-5,6,7,8-tetrahydro-3H-benzo[4,5]thieno[2,3-d]pyrimidin-4-one

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