methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

Base Information

Chemical Name:methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate
CAS No.:1174151-05-3
Molecular Formula:C₂₅H₂₇NO₇
Molecular Weight:453.492
Hs Code.:

Synonyms:methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

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Technology Process of methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

There total 1 articles about methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1174151-07-5
C₂₇H₃₃NO₈

: 1174151-05-3
methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

Guidance literature:: With sodium periodate; sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 20h;
DOI:10.1016/j.tet.2009.03.103

Reference yield:

: 1174151-05-3
methyl (R,E)-2-(benzyloxymethyl)-2-(N-(4-methoxybenzyl)-4-oxobut-2-enamido)-3-oxobutanoate

: 1055312-48-5
(3aS,6R,6aR)-6-benzyloxymethyl-5-(4-methoxybenzyl)-6a-methyl-2,4-dioxohexahydrofuro[2,3-c]pyrrole-6-carboxylic acid methyl ester

: 1055312-47-4
(3aR,6R,6aS)-6-benzyloxymethyl-5-(4-methoxybenzyl)-6a-methyl-2,4-dioxohexahydrofuro[2,3-c]pyrrole-6-carboxylic acid methyl ester

Guidance literature:: With C₂₆H₂₆N₃O⁽¹⁺⁾*Cl^(1-); 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; tert-butyl alcohol; at 40 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.103