C₂₈H₄₉NO₇Si₂

Base Information

Chemical Name:C₂₈H₄₉NO₇Si₂
CAS No.:1033588-35-0
Molecular Formula:C₂₈H₄₉NO₇Si₂
Molecular Weight:567.871
Hs Code.:

C<sub>28</sub>H<sub>49</sub>NO<sub>7</sub>Si<sub>2</sub>

Synonyms:C₂₈H₄₉NO₇Si₂

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Chemical Property of C₂₈H₄₉NO₇Si₂

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Technology Process of C₂₈H₄₉NO₇Si₂

There total 2 articles about C₂₈H₄₉NO₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1033588-33-8
C₂₁H₄₆O₄Si₂

: 62-23-7
4-nitro-benzoic acid

: 1033588-35-0
C₂₈H₄₉NO₇Si₂

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja803012n

Reference yield:

: 1033588-32-7
C₂₇H₆₀O₄Si₃

: 1033588-35-0
C₂₈H₄₉NO₇Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / tetrahydrofuran / 12 h / 0 - 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 °C

With water; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; 2: |Mitsunobu Displacement;
DOI:10.1021/jo3026077

Reference yield:

: 1033588-35-0
C₂₈H₄₉NO₇Si₂

: 1033588-21-4
C₃₈H₅₅NO₁₀Se

Guidance literature:: Multi-step reaction with 12 steps

1.1: methanol; barium hydroxide octahydrate / 4 h / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

3.2: -78 - -40 °C / Inert atmosphere

3.3: 0.5 h / -40 °C / Inert atmosphere

4.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

5.1: water; acetic acid / tetrahydrofuran / 5 h / -20 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 12 h / 20 °C / Inert atmosphere

6.2: 19 h / 20 °C / Inert atmosphere

7.1: methanol; barium hydroxide octahydrate / 0.33 h / 20 °C

8.1: tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C

8.2: 24 h / 20 °C

9.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran; dichloromethane; toluene / 0.75 h / -20 °C / Inert atmosphere

10.1: titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 5 h / -20 °C / Molecular sieve; Inert atmosphere

11.1: tributylphosphine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

12.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride; water / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; dmap; tetrapropylammonium perruthennate; barium hydroxide octahydrate; tributylphosphine; dimethylsulfide borane complex; 2,4,6-trichlorobenzoyl chloride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; acetic acid; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; In tetrahydrofuran; decane; dichloromethane; N,N-dimethyl-formamide; toluene; 10.1: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo3026077