ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate

Base Information

• Chemical Name: ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate
• CAS No.: 171051-11-9
• Molecular Formula: C₃₁H₃₃N₅O₄
• Molecular Weight: 539.634

Synonyms:ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate

Chemical Property of ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate

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Technology Process of ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate

There total 2 articles about ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

HCl*H-MeβAla-OEt + 3-[2-(2-Carboxymethyl-1-cyclohexenyl)-3-oxo-2,3-dihydropyridazin-6-yl]-2-phenylpyrazolo[1,5-a]-pyridine (171050-45-6) → ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate (171051-11-9)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; dichloromethane; at 20 ℃;

DOI:10.1016/S0968-0896(99)00258-8

Reference yield:

→ ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate (171051-11-9)

Guidance literature:

Reference yield: 80.0%

ethyl 3-[methyl-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetyl]amino]propionate (171051-11-9) → 3-(2-{2-(N-(2-carboxyethyl)-N-methylcarbamoyl)methyl-1-cyclohexenyl}-3-oxo-2,3-dihydropyridazin-6-yl)-2-phenylpyrazolo[1,5-a]pyridine

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃;

DOI:10.1016/S0968-0896(99)00258-8

upstream raw materials:

3-[2-(2-Carboxymethyl-1-cyclohexenyl)-3-oxo-2,3-dihydropyridazin-6-yl]-2-phenylpyrazolo[1,5-a]-pyridine

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