3,3-bis--1-propene

Base Information

Chemical Name:3,3-bis--1-propene
CAS No.:160968-58-1
Molecular Formula:C₂₇H₃₄O₄
Molecular Weight:422.565
Hs Code.:

3,3-bis-<trans-5-(4-methoxyphenyl)-2-pentenyloxy>-1-propene

Synonyms:3,3-bis--1-propene

Suppliers and Price of 3,3-bis--1-propene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-bis--1-propene

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Technology Process of 3,3-bis--1-propene

There total 3 articles about 3,3-bis--1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 160968-51-4
trans-5-(4-methoxyphenyl)-1-(trimethylsilyloxy)-2-pentene

: 107-02-8,25068-14-8
acrolein

: 160968-58-1
3,3-bis--1-propene

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In toluene; at -78 ℃; for 3h;
DOI:10.1016/S0040-4020(01)90391-6

Reference yield:

: 5-(4-Methoxy-phenyl)-pent-2-yn-1-ol

: 160968-58-1
3,3-bis--1-propene

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / LiAlH₄ / tetrahydrofuran / 18 h / Ambient temperature

2: 95 percent / imidazole / CH₂Cl₂ / 16 h / Ambient temperature

3: 26 percent / TMSOTf / toluene / 3 h / -78 °C

With 1H-imidazole; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)90391-6

Reference yield:

: 160968-45-6
(2E)-5-(4-methoxyphenyl)-2-penten-1-ol

: 160968-58-1
3,3-bis--1-propene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / imidazole / CH₂Cl₂ / 16 h / Ambient temperature

2: 26 percent / TMSOTf / toluene / 3 h / -78 °C

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)90391-6