(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

Base Information

Chemical Name:(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester
CAS No.:118896-76-7
Molecular Formula:C₁₉H₁₉N₃O₂
Molecular Weight:321.379
Hs Code.:

Synonyms:(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

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Chemical Property of (E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

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Technology Process of (E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

There total 3 articles about (E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 63613-50-3
benzyl 2-(tripheny l-λ5phosphanylidene)propanoate

: 118896-48-3
2-<(1H-imidazol-1-yl)methyl>-5-formylpyrrole

: 118896-76-7
(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

Guidance literature:: In acetonitrile; Heating;
DOI:10.1021/jm00124a027

Reference yield:

: 14745-84-7
2-(N,N-dimethylaminomethyl)pyrrole

: 118896-76-7
(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / xylene / 6 h / Heating

2: 1) POCl₃ / 1) r.t., 30 min, 2) DMF, 80 deg C

3: 75 percent / acetonitrile / Heating

With trichlorophosphate; In acetonitrile; xylene;
DOI:10.1021/jm00124a027

Reference yield:

: 76660-67-8
2-<(1H-imidazol-1-yl)methyl>pyrrole

: 118896-76-7
(E)-3-(5-Imidazol-1-ylmethyl-1H-pyrrol-2-yl)-2-methyl-acrylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) POCl₃ / 1) r.t., 30 min, 2) DMF, 80 deg C

2: 75 percent / acetonitrile / Heating

With trichlorophosphate; In acetonitrile;
DOI:10.1021/jm00124a027