ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Base Information

Chemical Name:ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate
CAS No.:75971-36-7
Molecular Formula:C₂₁H₂₆FN₅O₂S
Molecular Weight:431.534
Hs Code.:

Synonyms:ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Suppliers and Price of ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

There total 4 articles about ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 73733-70-7
ethyl 4-isothiocyanato-1-piperidinecarboxylate

: 73733-75-2
N²-<(4-fluorophenyl)methyl>-2,3-pyridinamine

: 75971-36-7
ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Guidance literature:: In methanol; for 2h; Heating;
DOI:10.1021/jm00150a030

Reference yield:

: 73733-74-1
N-<(4-fluorophenyl)methyl>-3-nitro-2-pyridinamine

: 75971-36-7
ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / RaNi / methanol / 760 Torr / Ambient temperature

2: 54 percent / methanol / 2 h / Heating

With hydrogen; RaNi; In methanol;
DOI:10.1021/jm00150a030

Reference yield:

: 5470-18-8,34515-82-7
2-Chloro-3-nitropyridine

: 75971-36-7
ethyl 4-<<<<2-<<(4-fluorophenyl)methyl>amino>-3-pyridinyl>amino>thioxomethyl>amino>-1-piperidine carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / sodium carbonate / dimethylformamide / 1 h / 90 °C

2: 100 percent / H₂ / RaNi / methanol / 760 Torr / Ambient temperature

3: 54 percent / methanol / 2 h / Heating

With hydrogen; sodium carbonate; RaNi; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00150a030