6--5,8-quinolinedione

Base Information

• Chemical Name: 6--5,8-quinolinedione
• CAS No.: 107127-71-9
• Molecular Formula: C₁₇H₁₅N₃O₂
• Molecular Weight: 293.325
• Mol file: 107127-71-9.mol

Synonyms:6--5,8-quinolinedione

Chemical Property of 6--5,8-quinolinedione

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 6--5,8-quinolinedione

There total 2 articles about 6--5,8-quinolinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

5,8-quinolinedione (10470-83-4) + 4-amino-N,N-dimethylaniline (99-98-9) → 6--5,8-quinolinedione (107127-71-9)

Guidance literature:

With oxygen; nickel dichloride; In ethanol; at 30 ℃; for 2h;

DOI:10.1246/cl.1986.1059

Reference yield: 43.0%

5,8-quinolinedione (10470-83-4) + 4-amino-N,N-dimethylaniline (99-98-9) → 7--5,8-quinolinedione (107127-72-0) + 6--5,8-quinolinedione (107127-71-9)

Guidance literature:

With oxygen; In ethanol; at 30 ℃; for 6h;

DOI:10.1246/cl.1986.1059

Reference yield:

copper(II) perchlorate hexahydrate + 6--5,8-quinolinedione (107127-71-9) → (6-(4-dimethylaminophenylamino)-5,8-quinolinedione)2copper(II) perchlorate

Guidance literature:

In ethanol; Addn. of metal salt soln. to soln. of ligand, stirring (room temp., 1 h).; Concg. in vac., cooling overnight in a refrigerator, filtn., drying in vac. over P2O5.;

DOI:10.1246/cl.1987.2057

upstream raw materials:

5,8-quinolinedione

4-amino-N,N-dimethylaniline