C₅₀H₆₉N₃O₁₃SSi

Base Information

Chemical Name:C₅₀H₆₉N₃O₁₃SSi
CAS No.:141823-81-6
Molecular Formula:C₅₀H₆₉N₃O₁₃SSi
Molecular Weight:980.262
Hs Code.:

C<sub>50</sub>H<sub>69</sub>N<sub>3</sub>O<sub>13</sub>SSi

Synonyms:C₅₀H₆₉N₃O₁₃SSi

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Chemical Property of C₅₀H₆₉N₃O₁₃SSi

Chemical Property:

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Technology Process of C₅₀H₆₉N₃O₁₃SSi

There total 14 articles about C₅₀H₆₉N₃O₁₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 141823-81-6
C₅₀H₆₉N₃O₁₃SSi

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

2: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

3: 86 percent / acetonitrile / 1.5 h / 25 °C

4: 100 percent / toluene / 1 h / 100 °C

5: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

6: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

7: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium tri-sec-butyl-borohydride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; sodium thiomethoxide; In dichloromethane; toluene; acetonitrile;

Reference yield:

: 126900-87-6
3-Chloro-benzoic acid (2S,3R,6R)-2-aminooxy-4-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3,6-dihydro-2H-pyran-3-yl ester

: 141823-81-6
C₅₀H₆₉N₃O₁₃SSi

Guidance literature:: Multi-step reaction with 8 steps

1: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

3: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

4: 86 percent / acetonitrile / 1.5 h / 25 °C

5: 100 percent / toluene / 1 h / 100 °C

6: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

7: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

8: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium tri-sec-butyl-borohydride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; sodium thiomethoxide; In dichloromethane; toluene; acetonitrile; benzene;

Reference yield:

: 132938-43-3
(3aS,4R,6R,7R,7aR)-7-Hydroxy-4-methyl-6-(2-nitro-benzyloxy)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-2-one

: 141823-81-6
C₅₀H₆₉N₃O₁₃SSi

Guidance literature:: Multi-step reaction with 11 steps

1: AgClO₄, SnCl₂, molecular sieves (4 Angstroem) / tetrahydrofuran / 7 h / -78 - -20 °C

2: NaH / tetrahydrofuran; ethane-1,2-diol / 0.5 h / 25 °C

3: 1.) n-Bu₂SnO, 2.) n-Bu₃SnOMe, Br₂ / 1.) MeOH, reflux, 1.2 h, 2.) CH₂Cl₂, 25 deg C

4: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

5: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

6: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

7: 86 percent / acetonitrile / 1.5 h / 25 °C

8: 100 percent / toluene / 1 h / 100 °C

9: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

10: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

11: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

With 2,6-dimethylpyridine; 4 A molecular sieve; tetrabutyl ammonium fluoride; bromine; tributyltin methoxide; silver perchlorate; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; di(n-butyl)tin oxide; potassium tri-sec-butyl-borohydride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; tin(ll) chloride; sodium thiomethoxide; In tetrahydrofuran; dichloromethane; ethylene glycol; toluene; acetonitrile; benzene;