8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one

Base Information

• Chemical Name: 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one
• CAS No.: 935756-22-2
• Molecular Formula: C₃₆H₃₀Cl₂N₄O₂
• Molecular Weight: 621.566

Synonyms:8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one

Chemical Property of 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one

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Technology Process of 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one

There total 2 articles about 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

p-chlorophenyl isocyanide (1885-81-0) + 1,7,8-triaza-3,3,6,6-tetramethyl-5-oxa-2-oxo-1-phenylspiro<3,4>oct-7-ene (134209-90-8) → 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one (935756-22-2)

Guidance literature:

In 1,1,2-trichloroethane; for 6h; Heating;

DOI:10.1021/jo0700631

Reference yield:

1,7,8-triaza-3,3,6,6-tetramethyl-5-oxa-2-oxo-1-phenylspiro<3,4>oct-7-ene (134209-90-8) → 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one (935756-22-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / dioxane / 11 h / Heating

2: 98 percent / 1,1,2-trichloro-ethane / 3 h / Heating

In 1,4-dioxane; 1,1,2-trichloroethane;

DOI:10.1021/jo0700631

Reference yield: 82.0%

8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-4-phenylimino-5-(3,3-dimethyl-1-phenylazetidin-2-on-4-yl)-δ-carbolin-2-one (935756-22-2) → 8-chloro-1-(p-chlorophenyl)-3,3-dimethyl-δ-carboline-2,4-dione

Guidance literature:

With toluene-4-sulfonic acid; In 1,1,2-trichloroethane; for 2h; Heating;

DOI:10.1021/jo0700631

upstream raw materials:

p-chlorophenyl isocyanide

1,7,8-triaza-3,3,6,6-tetramethyl-5-oxa-2-oxo-1-phenylspiro<3,4>oct-7-ene

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