(Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine

Base Information

• Chemical Name: (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine
• CAS No.: 1033036-89-3
• Molecular Formula: C₃₂H₄₉ClO₄Si₂
• Molecular Weight: 589.363

Synonyms:(Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine

Chemical Property of (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine

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Technology Process of (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine

There total 1 articles about (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

(Z,3S,8R,9R)-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2-hydroxymethyl-2,3,4,7,8,9-hexahydro-oxonine + t-butyldimethylsiyl triflate (69739-34-0) → (Z,2R,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine (1033036-91-7) + (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine (1033036-89-3)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 0.5h; Reflux;

DOI:10.1002/chem.200701567

Reference yield: 88.0%

(Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-hydroxy-2,3,4,7,8,9-hexahydro-oxonine (1033036-89-3) + O-(4-methoxybenzyl)-trichloroacetimidate (89238-99-3) → (Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-(4-methoxybenzyloxy)-2,3,4,7,8,9-hexahydro-oxonine (1033037-14-7)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In toluene; for 0.5h;

DOI:10.1002/chem.200701567

upstream raw materials:

t-butyldimethylsiyl triflate

Downstream raw materials:

(Z,2S,3S,8R,9R)-2-tert-butyldimethylsilanyloxymethyl-9-tert-butyldiphenylsilanyloxymethyl-8-chloro-3-(4-methoxybenzyloxy)-2,3,4,7,8,9-hexahydro-oxonine

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