C₁₄H₁₇NO

Base Information

Chemical Name:C₁₄H₁₇NO
CAS No.:1380225-15-9
Molecular Formula:C₁₄H₁₇NO
Molecular Weight:215.295
Hs Code.:

Synonyms:C₁₄H₁₇NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₇NO

Chemical Property:

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Technology Process of C₁₄H₁₇NO

There total 2 articles about C₁₄H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1380225-14-8
1,1,1-triisopropyl-N-(2-methylbuta-1,3-dien-1-ylidene)silanamine

: 1380225-15-9
C₁₄H₁₇NO

Guidance literature:: 3-phenyl-propionaldehyde; With tetrachlorosilane; Denmark's dimeric catalyst; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - -72 ℃; for 0.0833333h; Inert atmosphere;

1,1,1-triisopropyl-N-(2-methylbuta-1,3-dien-1-ylidene)silanamine; In dichloromethane; at -55 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201108795

Reference yield:

: 16529-56-9
2-METHYL-3-BUTENENITRILE

: 1380225-15-9
C₁₄H₁₇NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.13 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 °C / Inert atmosphere

2.1: Denmark's dimeric catalyst; tetrachlorosilane; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / -78 - -72 °C / Inert atmosphere

2.2: 24 h / -55 °C / Inert atmosphere

With n-butyllithium; tetrachlorosilane; Denmark's dimeric catalyst; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201108795

Reference yield: 68.0%

: 1380225-15-9
C₁₄H₁₇NO

: 115346-55-9
(-)-(3S)-5-phenylpentane-1,3-diol

Guidance literature:: C₁₄H₁₇NO; With oxygen; ozone; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201108795