BzlGly-BzlAbu-Ile-OBzl

Base Information

Chemical Name:BzlGly-BzlAbu-Ile-OBzl
CAS No.:162457-60-5
Molecular Formula:C₃₃H₄₁N₃O₄
Molecular Weight:543.706
Hs Code.:

Synonyms:BzlGly-BzlAbu-Ile-OBzl

Suppliers and Price of BzlGly-BzlAbu-Ile-OBzl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BzlGly-BzlAbu-Ile-OBzl

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Technology Process of BzlGly-BzlAbu-Ile-OBzl

There total 10 articles about BzlGly-BzlAbu-Ile-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 162457-59-2
Boc-BzlGly-BzlAbu-Ile-OBzl

: 162457-60-5
BzlGly-BzlAbu-Ile-OBzl

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 21h; Ambient temperature;
DOI:10.1002/hlca.19940770424

Reference yield:

: 110353-57-6
benzyl N-benzyl-N-<(tert-butoxy)carbonyl>glycinate

: 162457-60-5
BzlGly-BzlAbu-Ile-OBzl

Guidance literature:: Multi-step reaction with 3 steps

1: 48.4 g / hydrogen / 10percent Pd/C / ethanol / 18 h

2: 73 percent / bis<2-oxooxazolidin-3-yl>phosphinic chloride, (i-Pr)2EtN / CH₂Cl₂ / 36 h / Ambient temperature

3: 98 percent / CF₃COOH / CH₂Cl₂ / 21 h / Ambient temperature

With hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1002/hlca.19940770424

Reference yield:

: N-benzyl glycin benzyl ester hydrochloride

: 162457-60-5
BzlGly-BzlAbu-Ile-OBzl

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Et₃N, 4-(dimethylamino)pyridine / acetonitrile / 0.5 h

2: 48.4 g / hydrogen / 10percent Pd/C / ethanol / 18 h

3: 73 percent / bis<2-oxooxazolidin-3-yl>phosphinic chloride, (i-Pr)2EtN / CH₂Cl₂ / 36 h / Ambient temperature

4: 98 percent / CF₃COOH / CH₂Cl₂ / 21 h / Ambient temperature

With dmap; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile;
DOI:10.1002/hlca.19940770424