C₁₇H₂₂O₆

Base Information

Chemical Name:C₁₇H₂₂O₆
CAS No.:1313375-24-4
Molecular Formula:C₁₇H₂₂O₆
Molecular Weight:322.358
Hs Code.:

C<sub>17</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:C₁₇H₂₂O₆

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Chemical Property of C₁₇H₂₂O₆

Chemical Property:

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Technology Process of C₁₇H₂₂O₆

There total 10 articles about C₁₇H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1313375-86-8
C₂₃H₂₈O₉

: 1313375-24-4
C₁₇H₂₂O₆

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;
DOI:10.1002/chem.201003402

Reference yield:

: C₃₀H₃₄O₈

: 1313375-24-4
C₁₇H₂₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.1: 1H-imidazole; sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / Reflux; Inert atmosphere

5.1: hydrogenchloride / ethanol; water / 3 h / Reflux; Inert atmosphere

6.1: pyridine / ethanol / 24 h / 20 °C / Inert atmosphere

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

8.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

9.1: sodium methylate / methanol / 20 °C

With pyridine; 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; tri-n-butyl-tin hydride; sodium methylate; palladium diacetate; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 8.1: Heck coupling / 9.1: Zemplen reaction;
DOI:10.1002/chem.201003402

Reference yield:

: 1313375-81-3
C₃₅H₄₂O₈S₂

: 1313375-24-4
C₁₇H₂₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / Reflux; Inert atmosphere

2: hydrogenchloride / ethanol; water / 3 h / Reflux; Inert atmosphere

3: pyridine / ethanol / 24 h / 20 °C / Inert atmosphere

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

5: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

6: sodium methylate / methanol / 20 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; tri-n-butyl-tin hydride; sodium methylate; palladium diacetate; sodium hydrogencarbonate; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5: Heck coupling / 6: Zemplen reaction;
DOI:10.1002/chem.201003402